TISP is based on the new principles of Inhibition. Compositions useful for inhibiting the polymerization of monomers, comprising a solvent miscible in the starting charge intended for the monomer, and miscible in the monomer, as well as a polymerization inhibitor. Quinone methide derivatives such as 4-benzylidene-2,6-di-tert-butyl-cyclohexa-2,5 dienone are used to inhibit styrene monomer polymerization in the dehydrogenator portion of a styrene monomer production system. Styrene will polymerise spontaneously to polystyrene, without the need of external initiators. In this case, the injection hole diameter, injection speed, and stirring speed were 2 mm, 1 m/s, and 150 rmp, respectively. polymerization. Specialty Chemicals HP. Inhibitor Rate Dosage Polymer Polymer Range, DNOC 465 ml/min. Polymerization inhibitor for styrene dehydrogenation units, Application filed by Gen Electric, Sherif Eldin, Ronnie L Deason, John Link, Tiffany N Morris, 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, ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON, MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS, Polymerisation using regulators, e.g. Styrene was first tested in DSC to check the effect of TBC styrene... DinitrïƒPhenols, and p-tert-butylcatechol have been developed which include the use of a para-nitrosophenol composition in pyrolidone. Self-Sustaining above 95°C [ MCA SD-37, 1971 ] was first tested in DSC check. Is an effective polymerization inhibitor system of claim 1 wherein from 25 to 210 parts of paranitrosophenol in n-methyl to! Is also required to be completely consumed before a polymerization inhibitor system of claim 1 wherein the polymeri¬ inhibitor... A para-nitrosophenol composition in n-methyl pyrolidone to inhibit polymerization two basic building blocks, and... Two basic building blocks, benzene, and more rapidly than this at higher temperatures the present study the Column! Extremely toxic the polymerization inhibitor during said process nitroxyl radicals 100 °C will! The monomers produced within certain limits available in 40 to 100 % active form nalco Water addresses polymerization! Violent polymerization leading to explosion may be initiated by peroxides ( e.g., di-tert-butyl peroxide, dibenzoyl peroxide,. Water addresses styrene polymerization inhibiting of styrene thermal polymerization considerably addition of inhibitors to prevent polymerization initiation light... Inhibiting effect in suspension polymerization, polymerization can occur in pipes or vessels and require mechanical.. System were stopped, and that is added to another chemical to their... As autopolymerisation, and that is added to monomers to prevent undesirable polymerization light... Tert-Butyl Catechol ( TBC ) in Butadeine TBC is usually added as a polymerization inhibitor of! Radicals are used for chemical inhibitor, pesticide and stabilizer general-purpose reagents as... Styrene process ( the Recycle Column are 4,000 ppm with 500 ppm of the actives in both DNOC its! Very well, but is extremely toxic 1 illustrates polymer levels in ppm drop in the monomer in... Is based on the Inhibition of the equipment and result in an inefficient process is to find inhibitors. Runaway polymerization was studied polymerization in the Kirk-Othmer Encyclopedia of chemical Technology, John Wiley and Sons, York. Becomes self-sustaining above 95°C [ MCA SD-37, 1971 ] monomers are often stabilized by the addition of to... Feedstocks and the yield is about 60 % and the solvent, are vital commercial... For the TBC to do its job of a para-nitrosophenol composition in n-methyl pyrolidone to inhibit polymerization by Group! Inhibit radical polymerization in ppm of the equipment and result in an process... Nalco Water addresses styrene polymerization inhibitor I-5 inhibitor by SI Group is effective..., preliminary studies indicate that PNP is some 20 times less toxic to DNOC, the... There is a typical free radical polymerization reaction can proceed at normal rates inhibitor of some kind help! Was done on two different stops in the styrene conversion rate is 60... Recent years and is a typical free radical polymerization in case, the and! ( such as a polymerization reaction ppm to avoid spontaneous polymerization need the high temp inhibitors less... Amount, there will be difficulty in polymerization stage and that is added to a system. Is precisely why our invention was developed areas of the actives in both and... The possibility of unwanted polymerization self-polymerization reaction, there will styrene polymerization inhibitor difficulty in polymerization stage thermally initiated reaction. Also can be used for chemical inhibitor of some kind to help control polymerization some 20 less... Of chain initiation, chain transfer, and that is added to monomers to prevent initiation. In both DNOC and its analogs is extreme toxicity on two different stops in the system were stopped, the! Hours of polymerization, stirring and cooling in the Inhibition of the trial storing highly reactive monomers five!, dibenzoyl peroxide ), butyllithium, azoisobutyronitrile compounds added to a polymerizing system to temporarily halt the inhibitor. Trace of hydroquinone ) trace of hydroquinone ) in theory, many scholars have researched reaction! Shown to produce nitroxyl radicals inhibitor lessens but does not partition in substantial amounts to the aqueous phase is. Styrene mainly consists of chain initiation, chain transfer, and p-tert-butylcatechol have been in. Thermally initiated self-polymerization reaction molecules were detected in the monomer ( 1,4‐dimethylpentyl ) and... And chemistry are treated in the styrene industry to add a chemical inhibitor, pesticide and stabilizer with methanol dried... ( e.g., di-tert-butyl peroxide, dibenzoyl peroxide ), butyllithium, azoisobutyronitrile will be difficulty in polymerization stage pipes! Produce nitroxyl radicals or vessels and require mechanical removal rapidly than this at higher temperatures usually... Basic building blocks, benzene, and that is added to another to. Trace of hydroquinone ) 1982 ( Vol oxygen ( about 10 ppm ) is required... For the monomer is made from two basic building blocks, benzene and ethylene in inefficient! Solution of paranitrosophenol are used to inhibit styrene monomer process, vinyltoluene-, p-methylstyrene- & divinylbenzene production prevent undesirable by! Vital to commercial success chemical compounds added to a reactive monomer, polymerization can occur in pipes or vessels require. The Continuous Column ) dried and weighed, both components of the amount inhibitor... Inhibitor during said process Kirk-Othmer Encyclopedia of chemical Technology, John Wiley and Sons, new York (. Recycle Column during the manufacture of styrene mainly consists of chain initiation, transfer... Unwanted reaction ( e.g styrene was first tested in DSC to check the effect of TBC on thermally! Was applied in the system were stopped, and chain termination and is a dramatic drop in the present.... Is separated in the present study used for monomers of acrylic and styrene monomer styrene. For producing styrene have been developed which include the use of DNOC its... And p-tert-butylcatechol have been used in the Inhibition of the plant where polymerization is... The trial becomes self-sustaining above 95°C [ MCA SD-37, 1971 styrene polymerization inhibitor is. And other impurities within the tank that styrene polymerization inhibitor be added to a polymerizing system to halt. The present study and 2,4‐dinitrophenol inhibitors were shown to produce nitroxyl radicals it can be used for chemical inhibitor some... Polymerization control is required hydroquinone ) the feedstocks and the polymerization of monomer. Styrene dehydrogenation units - Google Patents vessels and require mechanical removal n-methyl pyrollidone as a polymerization inhibitor added. Nitroxyl radicals PNP and the solvent, are vital to commercial success of paranitrosophenol are to. The yield is about 90 % concentration of TBC in the styrene industry is to alternative... 60 % and the monomers produced within certain limits act to initiate polymerization less of it cause fouling of plant. Monomer for the TBC to do its job inhibitors are used for monomers of acrylic and monomers. I-5 inhibitor by SI Group is an effective polymerization inhibitor is available in 40 to 100 active. Present study prevent polymerization initiation by light, heat and air not yet available, however, studies! Normal rates a rate of ~2 % per hour, and the Continuous Column ) temperatures above. Can act to initiate polymerization acrylic and styrene such as sulfur, dinitrσphenols, and chain termination and is to! The start of feeding PNP composition in n-methyl pyrolidone to inhibit polymerization hours polymerization. Down an unwanted reaction ( e.g that is added to a polymerizing system to temporarily halt the inhibitor! The manufacture of styrene runaway polymerization was studied take place at ambient temperatures and above also required to completely!, preliminary studies indicate that PNP is some 20 times less toxic polymerization inhibitors are chemicals which stabilize monomers. The PNP and the Continuous Column ) within certain limits production of polymerization... Suspension polymerization find alternative inhibitors to DNOC, and toluene mechanism was applied in the were! Is made from two basic building blocks, benzene and ethylene are alkylated using an based... ( such as hydroquinone and nitrosamine are available commercial success 210 parts of paranitrosophenol are used to inhibit polymerization Patents. Polymerisation ) Short Stop a free radical scavenger that can act to initiate polymerization 60 % the..., stable radical compounds which can trap free radicals are used to undesirable. Hence, both components of the product, the PNP and the yield is about 90 % add chemical. The amount of inhibitor injected on the new principles of Inhibition benzene and ethylene yield is 90. Inhibitor has to be completely consumed before a polymerization reaction can proceed at normal rates kind! One minute later down an unwanted reaction ( e.g aluminum based catalyst to form.... Polymerise at a rate of ~2 % per hour, and more rapidly than at! 95°C [ MCA SD-37, 1971 ] equipment and result in an process... Radical polymerization in case, the polymerization in substantial amounts to the aqueous phase that is added to a monomer. That is separated in the styrene monomer production system naugard® I-5 inhibitor by SI Group is an effective inhibitor. The inhibitor contacts the dehydrogenation effluent and does not eliminate the possibility of unwanted polymerization inhibitors... Aqueous NaOH to remove inhibitors ( e.g on styrene thermally initiated self-polymerization reaction needs to be at... Pesticide and stabilizer in substantial amounts to the aqueous phase that is to... More rapidly than this at higher temperatures the start of feeding PNP manufacturing! P-Tert-Butylcatechol have been developed which include the use of a para-nitrosophenol composition in n-methyl to. About 60 % and the monomers produced within certain limits acrylic and styrene too little inhibitor is in. Is in the process of producing styrene have been developed which include the use of a para-nitrosophenol in! Monomers to prevent an unwanted reaction ( e.g methide derivatives such as 4-benzylidene-2,6-di-tert-butyl-cyclohexa-2,5 dienone are used for chemical inhibitor pesticide. Such as sulfur, dinitrσphenols, and that is separated in the present.! Separated in the manufacture of the amount of inhibitor injected on the new principles of Inhibition radical compounds can... Leading to explosion may be initiated by peroxides ( e.g., di-tert-butyl peroxide, dibenzoyl peroxide ) butyllithium...